Hydrochloric Acid → HCID 86584670, compound

Participants

Reaction Steps

Hydrogen chloride gas was passed through a stirred ice cold solution of tert-butyl 2-(dicyclopentylamino)ethylcarbamate (0.22 g, 0.74 mmol) (Preparation 52) in dichloromethane (15 ml) until the solution was saturated. The reaction mixture was allowed to warm to room temperature and then stirred for 1 hour. The solvent was removed under reduced pressure to give the title compound (0.15 g) as a brown foam.

Provenance & Evidence