HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-nitrophenol → 2-Amino-4,6-dichlorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-nitrophenol | HCID 11871 | — |
| Reactant | 2-Amino-6-chlorophenol | HCID 6486025 | — |
| Product | 2-Amino-4,6-dichlorophenol | HCID 10699 | — |
Reaction Steps
2-amino-4,6-dichlorophenol was prepared from 2,4-dichloro-6-nitrophenol (0.625 g, 2.40 mmol) in a manner similar to that described for 2-amino-6-chlorophenol. The compound was formed as a black solid (0.044 g, 10%). RP-HPLC (25 to 100% CH3CN in 0.1 N aqueous ammonium acetate over 10 min at 1 mL/min using a Hypersil HS C18, 100 Å, 5 μm, 250×4.6 mm column) tr=9.033 min., 74%; m/z 177 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06921763B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-d3b05d47f37b4e79b4c8ab532f2fba36 |
| Source note | uspto-grants-2005_07 |