HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(-)-2-Aminobutyric acid → (2S)-2-[(4-bromo-2-nitrophenyl)amino]butanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (-)-2-Aminobutyric acid | HCID 80283 | — |
| Edukt | 4-Bromo-1-fluoro-2-nitrobenzene | HCID 2736328 | — |
| Edukt | (R)-2-(4-fluoro-2-nitrophenylamino)-butyric acid | HCID 69223325 | — |
| Produkt | (2S)-2-[(4-bromo-2-nitrophenyl)amino]butanoic acid | HCID 69223203 | — |
Reaktionsschritte
5-Bromo-2-fluoronitrobenzene was treated with (S)-2-aminobutyric acid according to the procedure for the preparation of (R)-2-(4-fluoro-2-nitrophenylamino)-butyric acid (see Example 1) to yield (2S)-2-[(4-bromo-2-nitrophenyl)amino]butanoic acid. MS (ESI) m/z 303/305 ([M+H]+); MS (ESI) m/z 301/303 ([M−H]−).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07351709B2 |
| Quelldatensatz | uspto-grants-2008_04 |
| ORD ID | ord-bacfeb73b14e4160a2ea018572548031 |
| Quellennotiz | uspto-grants-2008_04 |