HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22261239, compound → HCID 22261187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22261239 | HCID 22261239 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22261187 | HCID 22261187 | 64% |
Reaction Steps
A solution of 4-[2-(4-benzyloxy-2-vinylphenoxy)ethyl]-5-methyl-2-phenyloxazole (1.30 g, 3.16 mmol) in ethanol (100 mL) was treated with 5% Pd/C (160 mg) and hydrogen (60 psi) at ambient temperature for 18 h. The mixture was filtered and concentrated in vacuo to give a tan solid (0.65 g, 64%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351728B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-f33b513e91de4a87a1844d09e2e81743 |
| Source note | uspto-grants-2008_04 |