HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-1-(2,2-diethoxy-ethoxy)4-nitrobenzene → 3-Chloro-4-(2,2-diethoxy-ethoxy)-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-1-(2,2-diethoxy-ethoxy)4-nitrobenzene | HCID 55247821 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Chloro-4-(2,2-diethoxy-ethoxy)-phenylamine | HCID 68875671 | — |
Reaction Steps
30 g (0.104 mol) of 2-chloro-1-(2,2-diethoxy-ethoxy)-4-nitrobenzene was added to a suspension of 1.50 g Pd/C (10%) in 500 mL EtOAc and the mixture was hydrogenated for 2 hours at 20 psi. The catalyst was filtered off and the filtrate evaporated down i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351719B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-71ed4315d90b4a50ae6f22d698881128 |
| Source note | uspto-grants-2008_04 |