HRID898522

反应详情

EQUATION

反应方程式

HRID 898522 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2.6 g (10.9 mmol) of diethyl-[2-(4-nitro-phenoxy)-ethyl]-amine was added to a suspension of 130 mg Pd/C (10%) in 20 mL MeOH and the mixture was hydrogenated for 4 hours. The catalyst was filtered off and the filtrate evaporated down i. vac.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. customthe filtrate evaporated down i