1-Chloro-2-(diethylamine)ethane hydrochloride → HCID 69313096, compound
Reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]([N+:13]([O-:15])=[O:14])=[C:6]([CH:12]=1)[C:7]([O:9][CH2:10][CH3:11])=[O:8].Cl.Cl[CH2:18][CH2:19][N:20]([CH2:23][CH3:24])[CH2:21][CH3:22]>>[N+:13]([C:5]1[CH:4]=[CH:3][C:2]([O:1][CH2:18][CH2:19][N:20]([CH2:23][CH3:24])[CH2:21][CH3:22])=[CH:12][C:6]=1[C:7]([O:9][CH2:10][CH3:11])=[O:8])([O-:15])=[O:14]Participants
3
Procedure
Prepared analogously to intermediate product Z5a from ethyl 5-hydroxy-2-nitrobenzoate and (2-chloroethyl)-diethyl-amine-hydrochloride
Workup
- customPrepared analogously to intermediate product
Sources & evidence
- ORD record
- ord-51d5e5d25af0484e927ab073b8e53597
- Source dataset
- uspto-grants-2008_04
- Patent number
- US07351719B2
Reaction notes
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