HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
[2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine → [2-(3-Chloro-4-aminophenoxy)ethyl]diethylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine | HCID 68816613 | — |
| Katalysator | Nickel | HCID 935 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | [2-(3-Chloro-4-aminophenoxy)ethyl]diethylamine | HCID 57082476 | — |
Reaktionsschritte
A suspension of 1.24 g (4.547 mmol) [2-(3-chloro-4-nitro-phenoxy)-ethyl]diethyl-amine (Z27a) and 300 mg Raney nickel in EtOAc was hydrogenated at RT and 3 bar. The catalyst was filtered off and the filtrate evaporated down i. vac.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07351719B2 |
| Quelldatensatz | uspto-grants-2008_04 |
| ORD ID | ord-54eabcce50c24f09a57bf0eab15f9a0e |
| Quellennotiz | uspto-grants-2008_04 |