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HRID898625

反应详情

EQUATION

反应方程式

HRID 898625 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(CN2CCCCC2)cc1
HCID846150

4-(piperidin-1-ylmethyl)aniline

C12H18N2

结构：O=C(O)/C=C/c1ccc(-c2ccc(Cl)cc2)cn1
HCID59691634

未命名化合物

PRODUCTS

生成物

1
结构：O=C(/C=C/c1ccc(-c2ccc(Cl)cc2)cn1)Nc1ccc(CN2CCCCC2)cc1
HCID59691558

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 143 starting from (E)-3-[5-(4-chloro-phenyl)-pyridin-2-yl]-acrylic acid (Z34b) and 4-piperidin-1-ylmethyl-phenylamine. The crude product was purified by column chromatography (silica gel, dichloromethane/EtOH/conc. aqueous ammonia 50:10:0.1).

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (silica gel, dichloromethane/EtOH/conc. aqueous ammonia 50:10:0.1)