HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → Tert-butyl 3-oxopyrrolidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | tert-Butyl (3R)-3-hydroxypyrrolidine-1-carboxylate | HCID 6544479 | — |
| Product | Tert-butyl 3-oxopyrrolidine-1-carboxylate | HCID 471360 | — |
Reaction Steps
Prepared from (R)-(+)-1-Boc-3-pyrrolidinol using the Dess-Martin oxidation (Dess, D. B.; Martin, J. C.; J. Am. Chem. Soc., 1991, 113, 7277) (85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351822B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-080fb3d8194640e8a14048e9dc6ddcb6 |
| Source note | uspto-grants-2008_04 |