4-Nitrophenylboronic acid → HCID 11232672, compound

HRID 899216Notes

Reaction equation

HRID 899216 reaction equation
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:14])([CH3:13])[C:6]=2[CH:15]=1.[N+:16]([C:19]1[CH:24]=[CH:23][C:22](B(O)O)=[CH:21][CH:20]=1)([O-:18])=[O:17]>>[CH3:11][N:10]1[C:5]2[CH:4]=[CH:3][C:2]([NH:1][C:22]3[CH:23]=[CH:24][C:19]([N+:16]([O-:18])=[O:17])=[CH:20][CH:21]=3)=[CH:15][C:6]=2[C:7]([CH3:13])([CH3:14])[O:8][C:9]1=[O:12]

Participants

3

Reactant 2

HCID 27735524-Nitrophenylboronic acidHCID 69215309HCID 69215309, compound

Product 1

HCID 11232672HCID 11232672, compound

Procedure

Prepared from 6-amino-1,4,4-trimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one and 4-nitrophenyl boronic acid according to the coupling procedure described in example 1. MS (ESI) m/z 328 ([M+H]+); MS (ESI) m/z 326 ([M−H]−); Anal. calcd for C17H17N3O4: C, 62.38; H, 5.23; N, 12.84. Found: C, 62.03; H, 5.15; N, 11.41.

Sources & evidence

ORD record
ord-735c271de0c34cf785fea6331f741fcd
Source dataset
uspto-grants-2008_04
Patent number
US07354915B2

Reaction notes

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