4-(Dimethylamino)phenylboronic acid → HCID 11404603, compound

HRID 899236Notes

Reaction equation

HRID 899236 reaction equation
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:14])([CH3:13])[C:6]=2[CH:15]=1.[CH3:16][N:17]([CH3:27])[C:18]1[CH:23]=[CH:22][C:21](B(O)O)=[CH:20][CH:19]=1>>[CH3:16][N:17]([CH3:27])[C:18]1[CH:23]=[CH:22][C:21]([NH:1][C:2]2[CH:3]=[CH:4][C:5]3[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:13])([CH3:14])[C:6]=3[CH:15]=2)=[CH:20][CH:19]=1

Participants

3

Procedure

Prepared from 6-amino-1,4,4-trimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one and 4-dimethylaminophenyl boronic acid according to the coupling procedure described in example 1. MS (ESI) m/z [M+H]+(326).

Sources & evidence

ORD record
ord-90fab6fee9314b50a94c09d94c4c7591
Source dataset
uspto-grants-2008_04
Patent number
US07354915B2

Reaction notes

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