HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 17956301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 17956302 | HCID 17956302 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17956301 | HCID 17956301 | 85.8% |
Reaction Steps
A stirred solution of the product of step (c) (16 g) and 10% palladium on carbon (1 g) in 1:1 acetic acid:ethanol (150 ml) was placed under an atmosphere of hydrogen at 20° C. for 24 hours. The reaction mixture was filtered through a pad of celite and the solvent removed in vacuo to give the title compound (11 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07354966B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-e58d9cb173a3441b878cd535c75206e7 |
| Source note | uspto-grants-2008_04 |