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HRID899478

反应详情

EQUATION

反应方程式

HRID 899478 的结构方程式

REACTANTS

反应物

3
结构：CCCN(c1cc(COCC(C)(N)Cc2ccccc2)cc(C(=O)N2CCCC2c2ccccc2)c1)S(C)(=O)=O
HCID11215160

未命名化合物

结构：CC#CC(C)N
HCID20392430

未命名化合物

2 次

结构：CCCN(c1cc(COCC(C)(Cc2ccccc2)NC(=O)OC(C)(C)C)cc(C(=O)O)c1)S(C)(=O)=O
HCID58856337

未命名化合物

2 次

PRODUCTS

生成物

1
结构：CC#CC(C)NC(=O)c1cc(COCC(C)(N)Cc2ccccc2)cc(N(CCC)S(C)(=O)=O)c1
HCID11443409

未命名化合物

PROCEDURE

实验过程

3-[(2-amino-2-methyl-3-phenylpropoxy)methyl]-N-(1-methylbut-2-yn-1-yl)-5-[(methylsulfonyl)(propyl)amino]benzamide was prepared from 3-({2-[(tert-butoxycarbonyl)amino]-2-methyl-3-phenylpropoxy}methyl)-5-[(methylsulfonyl)(propyl)amino]benzoic acid (intermediate XI) and (1-methylbut-2-yn-1-yl)amine (intermediate XIII) following a similar procedure as described for the preparation of N-{3-[(2-amino-2-methyl-3-phenylpropoxy)methyl]-5-[(2-phenylpyrrolidin-1-yl)carbonyl]phenyl}-N-propylmethanesulfonamide. HRMS (ES, M+H) calculated for C27H37N3O4S: 500.2578, found: 500.2595.