3-Phenylphenol → HCID 11483251, compound

HRID 899515Notes

Reaction equation

HRID 899515 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O:15][C:16]([C:18]1[O:19][C:20]([CH2:23]Cl)=[CH:21][CH:22]=1)=[O:17]>>[C:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:12]=[CH:11][CH:10]=[C:9]([O:13][CH2:23][C:20]2[O:19][C:18]([C:16]([OH:17])=[O:15])=[CH:22][CH:21]=2)[CH:8]=1

Participants

3

Reactant 2

HCID 113813-PhenylphenolHCID 75065Methyl 5-(chloromethyl)-2-furoate

Product 1

HCID 11483251HCID 11483251, compound

Procedure

5-(Biphenyl-3-yloxymethyl)-furan-2-carboxylic acid was prepared using general procedure A from 3-phenylphenol (available from Aldrich, Milwaukee, Wis.) and 5-chloromethylfuran-2-carboxylic acid methyl ester (available from Aldrich, Milwaukee, Wis., or from Maybridge plc, Tintagel, UK). Yield: 67 mg. Mass spectrum (ES) MH+=295.

Sources & evidence

ORD record
ord-5aca3921ec694e059f4c5e150251a9d4
Source dataset
uspto-grants-2008_04
Patent number
US07355049B2

Reaction notes

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