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HRID899944

反应详情

EQUATION

反应方程式

HRID 899944 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccncc1
HCID13389

Pyridin-4-carboxaldehyde

C6H5NO

结构：Nc1ccc(S(=O)(=O)C(F)(F)F)cc1
HCID136315

4-Aminophenyl trifluoromethyl sulphone

C7H6F3NO2S

结构：O=C(N[C@@H](CO)C(=O)O)OCC1c2ccccc2-c2ccccc21
HCID6541433

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H]1C(=O)N(c2ccc(S(=O)(=O)C(F)(F)F)cc2)C(=O)N1Cc1ccncc1.O=C(O)C(F)(F)F
HCID10346809

未命名化合物

PROCEDURE

实验过程

The compound is prepared from 0.025 mmol of resin, 0.075 mmol of N-Fmoc-L-Ala(OH), 0.125 mmol of 4-pyridinecarboxaldehyde and 0.0625 mmol of 4-(trifluoromethanesulfonyl)aniline, in the same way as in Example 1. After purification by preparative LC-MS, 5.6 mg of expected product are obtained.

WORKUP

后处理

  1. customAfter purification by preparative LC-MS, 5.6 mg of expected product
  2. customare obtained