HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Quinolinecarboxaldehyde → HCID 87565005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| Reactant | 4-Aminophenyl trifluoromethyl sulphone | HCID 136315 | — |
| Reactant | HCID 60112698 | HCID 60112698 | — |
| Product | HCID 87565005 | HCID 87565005 | 35.5% |
Reaction Steps
The compound is prepared from 4 mmol of resin, 12 mmol of N-Fmoc-Gly(OH), 20 mmol of 4-quinolinecarboxaldehyde, and 10 mmol of 4-(trifluoromethanesulfonyl)aniline, in the same way as in Example 1. After purification by preparative LC-MS, 1 g of expected product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07354933B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-12cbb1b96e7349bb9ca9eb3cbd7aa53d |
| Source note | uspto-grants-2008_04 |