HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → 1-Ethoxyethyl Methacrylate (stabilized with MEHQ)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Product | 1-Ethoxyethyl Methacrylate (stabilized with MEHQ) | HCID 20193345 | 80% |
Reaction Steps
To a mixture of 1.00 g of methacrylic acid and 0.836 g of ethyl vinyl ether was added 2 mg of p-toluenesulfonic acid monohydrate, and a reaction was allowed at room temperature for 1 hour. The conversion ratio of methacrylic acid was 82%, with the conversion ratio of ethyl vinyl ether of 94%. Accordingly, 1-ethoxyethyl methacrylate was obtained with the reaction yield of 80% and the selection ratio to ethyl vinyl ether of 85%, and a polymer of ethyl vinyl ether was produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358030B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-069a77f2b55e4a538d01927f9f4c4b4b |
| Source note | uspto-grants-2008_04 |