HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 22234832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 1-ethoxy-2-methylpropene | HCID 11051587 | — |
| Catalyst | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Product | HCID 22234832 | HCID 22234832 | 67.8% |
Reaction Steps
In 5.00 g of toluene were dissolved 1.00 g of phenol, 2.12 g of 1-ethoxy-2-methylpropene and 27 mg of a p-toluenesulfonic acid pyridinium salt, and a reaction was allowed at room temperature for 15 hours. After distilling toluene out from the reaction mixture under a reduced pressure, the concentrated residue was purified on a silica gel chromatography to give 1.40 g of 1-ethoxy-2-methylpropoxybenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358030B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-8caf01f8ccb1430aaeb69247ff1d0851 |
| Source note | uspto-grants-2008_04 |