HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-(2-Methyl-benzylidene)-pyrrolidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Methylbenzaldehyde | HCID 10722 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Product | 1-(2-Methyl-benzylidene)-pyrrolidinium chloride | HCID 17912280 | — |
Reaction Steps
The reaction of 8.2 ml (0.100 mol) pyrrolidine and 7.0 g (0.050 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 6.6 g (corresponding to 63% of the yield calculated by theory) 1-(2-methyl-benzylidene)-pyrrolidinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091220B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-d745609141254580931317ff1b8db479 |
| Source note | uspto-grants-2006_08 |