HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 3-ethynyl- → HCID 86607966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 3-ethynyl- | HCID 104682 | — |
| Reactant | HCID 68897788 | HCID 68897788 | — |
| Reactant | HCID 68900372 | HCID 68900372 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86607966 | HCID 86607966 | — |
Reaction Steps
Compound 18A was prepared from 15B and 3-ethynylaniline in a similar way as 15C. It has an analytical HPLC retention time=2.353 min (Chromolith SpeedROD column 4.6×50 mm, 10-90% aqueous methanol containing 0.1% TFA over 4 minutes, 4 mL/min, monitoring at 254 nm) and a LC/MS M++H=500+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358256B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-970aca6e260e4b65bbc9c6fcdb5367bb |
| Source note | uspto-grants-2008_04 |