HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86611141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfamic Acid | HCID 5987 | — |
| Reactant | HCID 58827600 | HCID 58827600 | — |
| Reactant | HCID 69291669 | HCID 69291669 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86611141 | HCID 86611141 | — |
Reaction Steps
The diazo solution obtained was added gradually to a stirred coupling mixture of N-ethyl, N-(2-cyanomethoxycarbonylethyl)-m-toluidine (7.3 parts), methanol (50 parts), water (200 parts) and sulphamic acid (1 part). After two hours the product was isolated by filtration, washed with cold water and dried to yield, 4-(4-nitrophenylazo)-3-methyl-N-ethyl-N-(2-cyanomethoxycarbonylethyl)aniline (6.5 parts) λmax=486 nm (acetone).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358345B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-027f6cec99d74bb9b474fd993502fbf7 |
| Source note | uspto-grants-2008_04 |