HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 571412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 1-Hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine | HCID 688178 | — |
| Product | HCID 571412 | HCID 571412 | 83% |
Reaction Steps
Using 1-hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine, prepared as described by: Kurumada T. et. al., loc. cit., and benzoyl chloride in a procedure otherwise similar to that for preparing the compound 101 gives an 83% yield of the compound 111 which is obtained in the form of colourless crystals; melting point. 138-140° C. (toluene/hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358365B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-84cd952623f340beb6521ed91029e93c |
| Source note | uspto-grants-2008_04 |