HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Methyl-2-furanethanol → 2-Propanone, 1-(2-furanyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Methyl-2-furanethanol | HCID 10855456 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Propanone, 1-(2-furanyl)- | HCID 228583 | — |
Reaction Steps
To a solution of 1-(2-furyl)-propan-2-ol (3.25 g) in dichloromethane (200 ml) was added in one portion pyridinium chlorochromate (13.0 g). The resulting mixture was stirred at room temperature for 5 h and then filtered through a small bed of silica. The organics were evaporated to give the crude product which was used without further purification (3.53 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358376B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4683adfa5749461e8b7a09aaf60e18b8 |
| Source note | uspto-grants-2008_04 |