HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 1-Benzylidene-pyrrolidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Product | 1-Benzylidene-pyrrolidinium chloride | HCID 10932360 | — |
Reaction Steps
The reaction of 16.4 ml (0.200 mol) pyrrolidine and 10.1 ml (0.100 mol) benzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 6.0 ml (0.100 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 14.1 g (corresponding to 72% of the yield calculated by theory) 1-benzylidene-pyrrolidinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091220B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-55eedef74ef9485e918bed4ebdb783d6 |
| Source note | uspto-grants-2006_08 |