HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 900684Generated: October 30, 2026
Potassium Carbonate → HCID 23117196, compound
https://huagongshe.com/reaction/900684
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (3-Bromopropoxy)(tert-butyl)dimethylsilane | HCID 607486 | — |
| Reactant | Ethyl 3-chloro-5-fluoro-4-hydroxybenzoate | HCID 23117176 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23117196 | HCID 23117196 | — |
Reaction Steps
Potassium carbonate and 3-(tert-butyldimethylsilyloxy)propyl bromide were added to a DMF solution of ethyl 3-chloro-5-fluoro-4-hydroxybenzoate, and the mixture was stirred at 50° C. to obtain ethyl 4-[3-(tert-butyldimethylsilyloxy)propoxy]-3-chloro-5-fluorobenzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07361658B2 |
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| Source dataset | uspto-grants-2008_04 |
|---|
| ORD ID | ord-ad88a06897cb44aabef403317988ff6a |
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| Source note | uspto-grants-2008_04 |
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