4-Benzylpiperidine → HCID 22350163, compound

HRID 900789Notes

Reaction equation

HRID 900789 reaction equation
[NH:1]1[C:12]2[C:4](=[CH:5][CH:6]=[C:7]3[C:11]=2[CH:10]=[CH:9][NH:8]3)[CH:3]=[C:2]1[C:13]([OH:15])=O.[CH2:16]([CH:23]1[CH2:28][CH2:27][NH:26][CH2:25][CH2:24]1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(OCC)C>[CH2:16]([CH:23]1[CH2:28][CH2:27][N:26]([C:13]([C:2]2[NH:1][C:12]3[C:4]([CH:3]=2)=[CH:5][CH:6]=[C:7]2[C:11]=3[CH:10]=[CH:9][NH:8]2)=[O:15])[CH2:25][CH2:24]1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

4

Reactant 2

HCID 317384-BenzylpiperidineHCID 22350203HCID 22350203, compound

Product 1

HCID 22350163HCID 22350163, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The title compound is prepared from 1,6-dihydro-1,6-diaza-as-indacene-2-carboxylic acid and 4-benzylpiperidine according to the method described in Example 1/c. Mp.: 186-188° C. (diethyl ether).

Sources & evidence

ORD record
ord-9b68a08bd31740508f7dcb0dd21772bf
Source dataset
uspto-grants-2008_04
Patent number
US07361670B2

Reaction notes

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