Potassium Iodide → HCID 22138019, compound

Participants

Reaction Steps

2-t-Butyl-9,10-bis(4-(2,2-diphenylvinyl)phenyl)-9,10-dihydroxy-9,10-dihydroanthracene (3.3 g, 4.3 mmole) was dissolved into acetic acid (30 ml). To the resultant solution, potassium iodide (1.9 g, 11 mmole, 2.7 eq) and sodium phosphinate monohydrate (0.6 g, 5.7 mmole) were added and the obtained mixture was stirred for 2 hours. The reaction mixture was filtered and washed with water, methanol and acetone and a light yellow solid (2.8 g, 88%) was obtained.

Provenance & Evidence