Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4,5-Trimethoxyaniline → N-(3,4,5-Trimethoxyphenyl)-4-(methylthio)benzenecarboximidamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4,5-Trimethoxyaniline | HCID 32285 | — |
| 반응물 | 4-(Methylthio)benzonitrile | HCID 590960 | — |
| 생성물 | N-(3,4,5-Trimethoxyphenyl)-4-(methylthio)benzenecarboximidamide | HCID 178493220 | — |
반응 단계
The title compound was prepared from 4-methylthiobenzonitrile (4.1 g, 27 mmol) and 3,4,5-trimethoxyaniline (5 g, 27 mmol) by following the procedure described in preparation 10 (7.8 g, yield 86.32%). 1H-NMR (CDCl3):δ 2.51 (s, 3H), 3.8 (s, 9H), 4.9 (bs, 2H, D2O exchangeable), 6.23 (s, 2H), 7.24-7.30 (m, 2H), 7.78-7.8 (d, 2H). MS m/z:333.5 (M+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07365069B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-60503023062e4b44b786bb3c4ee2f99c |
| 출처 메모 | uspto-grants-2008_04 |