HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → HCID 178503189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 4-(Methylthio)benzonitrile | HCID 590960 | — |
| Product | HCID 178503189 | HCID 178503189 | 77.7% |
Reaction Steps
The title compound was prepared from 4-methylthiobenzonitrile (17.3 g, 116 mmol) and 4-bromoaniline (20 g, 116 mmol) by following the procedure described in preparation 10 (29 g, yield 77.7%, purity 99.8% by HPLC). MS m/z:321.1/323.2 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365069B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4d6163f1474b45c28e432584801d2eb7 |
| Source note | uspto-grants-2008_04 |