P-Anisidine → HCID 178492294, compound

Participants

Reaction Steps

The title compound was prepared from 4-methylthiobenzonitrile (12.11 g, 81 mmol) and 4-methoxyaniline (10 g, 81 mmol) by following the procedure described in preparation 10 (17 g, yield 76.84%, mp 166-168° C., purity 97.25% by HPLC). 1H-NMR (CDCl3):δ 2.51 (s, 3H), 3.80 (s, 3H), 4.80 (bs, 2H, D2O exchangeable), 6.91 (s, 4H), 7.26-7.29 (m, 2H), 7.78-7.8 (d, 2H). IR (KBr) cm−1: 3461, 3320, 2949, 2922, 2829, 1615. MS m/z:273.1 (M+).

Provenance & Evidence