3-Cyanopyridine → HCID 178426510, compound

Participants

Reaction Steps

The title compound was prepared from 3-cyanopyridine (8.6 g, 83 mmol) and 3,4-dimetylaniline (10 g, 83 mmol) by following the procedure described in preparation 10 (15.6 g, yield 84%, mp 132-134 C, purity 99.7% by HPLC). 1H-NMR (CDCl3):δ 2.24-2.26 (d, 6H), 4.92 (bs, 2H, D2O exchangeable), 6.72-6.74 (d, 1H), 6.78 (s, 1H), 7.11-7.13 (d, 1H), 7.36-74 (m, 1H), 8.22-8.24 (d, 1H), 8.69-8.7 (d, 1H), 9.06 (d, 1H). IR (KBr) cm−1: 3313, 3142, 2997, 2958, 2918, 1651. MS m/z:226.1 (M+).

Provenance & Evidence