HCID 58646747, compound → HCID 69203352, compound

Participants

Reaction Steps

To a solution of trans 3-benzyloxycarbonylamino-2-hydroxy-1,2,3,4-tetrahydronaphthalene (850 mg) in dichloromethane (29 mL) stirring under nitrogen at room temperature was added pyridinium chlorochromate (740 mg). After 3 h, the reaction mixture was evaporated under vacuum onto silica gel and then purified by silica gel chromatography eluting with a step-wise gradient of 30-75% ethyl acetate in hexane to obtain the title compound (300 mg) as a white solid and starting material (350 mg).

Provenance & Evidence