Ethanethiol → HCID 135983747, compound

Participants

Reaction Steps

Add ethanethiol (6.8 mL, 92.5 mmol), followed by a sodium hydride (60% dispersion in mineral oil, 3.7 g, 92.5 mmol) to a solution of 7-methoxy-4-(2-pyridin-2-yl-pyrazolo[1,5-a]pyridin-3-yl)-quinoline (1.63 g, 4.6 mmol) in DMF (50 mL) at room temperature. Following the same procedure described above affords the title compound 0.8 g (52%) as a yellow solid.

Provenance & Evidence