Triethylamine → HCID 69038124, compound

Participants

Reaction Steps

To a solution of 60 mg 1H-Indazole-3,5-dicarboxylic acid 5-methyl ester and 52 mg 4-(4-Amino-phenyl)-morpholin-3-one in 2 mL DCM, 68 mg BOP-Cl and 0.15 mL NEt3 were added and the mixture was stirred for 16 h at RT. Then after the reaction mixture was diluted with 20 mL DCM, the solution was washed with 15 mL of water. The organic phase was dried over MgSO4 and after filtration concentrated under reduced pressure. The crude product was subjected to the next reaction step without further purification. Yield: 71 mg.

Provenance & Evidence