反应详情

N-Boc-N-propyl-N-propoxyamine (5.8 g) was dissolved in 4 N HCl/dioxane (10 mL) and stirred at room temperature for 7 hours. The solvent was removed in vacuo and the residue triturated with diethyl ether. The resulting yellow solid (2.1 g) was collected by filtration and washed with diethyl ether.

1. customThe solvent was removed in vacuo
2. customthe residue triturated with diethyl ether
3. filtrationThe resulting yellow solid (2.1 g) was collected by filtration
4. washwashed with diethyl ether