HuagongsheHuagongshe Chemistry Print Report · For research reference only
Mesitylene → HCID 68965446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Mesitylene | HCID 7947 | — |
| Reactant | HCID 69117900 | HCID 69117900 | — |
| Product | HCID 68965446 | HCID 68965446 | 75% |
Reaction Steps
A solution of 2-allyloxy-6-chloro-2′-methylbiphenyl (4.0 g, 15.4 mmol) in mesitylene (100 mL) was refluxed for 24 h. The solvent was removed under reduced pressure. Purification by ISCO using a solvent gradient of 0 to 20% ethyl acetate in hexanes provided 3.0 g (75%) of 3-allyl-6-chloro-2′-methylbiphenyl-2-ol as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-e4dfd4a6aeab4201805d80f06b3b130d |
| Source note | uspto-grants-2008_04 |