Allyl bromide → HCID 69118446, compound

Participants

Reaction Steps

Treatment of 5-fluoro-2′-phenylbiphenyl-2-ol (6.8 g, 25.7 mmol) with potassium carbonate (5.3 g, 38.6 mmol) and allyl bromide (3.3 mL, 38.6 mmol) in DMSO (150 mL) according to the procedure described for Example 69, Step 3 provided 6.4 g (82%) of 2-allyloxy-5-fluoro-2′-phenylbiphenyl as a white solid. MS (EI) m/z 304.1264 ([M]+); mp 48–49° C.

Provenance & Evidence