Potassium Bromide → HCID 11953163, compound

Participants

Reaction Steps

1,2-Bis(4-amino-3-hydroxyphenoxy)benzene was synthesized in a manner analogous to Example 2 from 1,2-bis(3-hydroxy-4-nitrophenoxy)benzene. Yield: 75.1%; mp>180° C. (decompose); IR (KBr): 3362, 3295, 3035, 1601 cm−1; MS (EI) m/z 324 (M+, 100); Elemental Anal. Calcd. for C18H16N2O4: C, 66.67; H, 4.94; N, 8.64. Found: C, 66.28; H, 5.04; N, 8.52.

Provenance & Evidence