HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Chloromethyl)benzoyl chloride → 2-Hydroxy-5-{[(3-methylbut-2-enoyl)(4-{[(4-pentylbenzyl)amino]carbonyl}-benzyl)amino]methyl}benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Chloromethyl)benzoyl chloride | HCID 70136 | — |
| Reactant | 3-Methyl-2-butenoyl chloride | HCID 102394 | — |
| Reactant | (4-Pentylphenyl)methanamine | HCID 2775785 | — |
| Reactant | 6-(aminomethyl)-2,2-dimethyl-4H-1,3-benzodioxin-4-one acetate | HCID 67420478 | — |
| Product | 2-Hydroxy-5-{[(3-methylbut-2-enoyl)(4-{[(4-pentylbenzyl)amino]carbonyl}-benzyl)amino]methyl}benzoic acid | HCID 11786063 | — |
Reaction Steps
The title compound was prepared following the procedure A using 4-pentylbenzylamine, 4-(chloromethyl)benzoyl chloride, 3-methylbut-2-enoyl chloride and 6-(aminomethyl)-2,2-dimethyl-4H-1,3-benzodioxin-4-one acetate. M+(ESI): 543.5
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365225B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-6ea6625a12f54ef3a5d18668bad41e44 |
| Source note | uspto-grants-2008_04 |