HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178504015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 12763849 | HCID 12763849 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178504015 | HCID 178504015 | — |
Reaction Steps
[1-(3-methylbutyl)-3-methyl-5-pyrazolyl]thiourea (23.0 g.) was dissolved in 250 ml. ethanol and 15.62 g. methyl iodide and refluxed for 4 hours. The ethanol was concentrated in vacuum and ether added to get 29.3 g. product, mp 128°-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226773 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-83bf5f2443904217abe057e7a4a18002 |
| Source note | uspto-grants-1980_10 |