Methyl iodide → HCID 178504016, compound

HRID 903049Notes

Reaction equation

HRID 903049 reaction equation
[CH3:1][N:2]1[C:6]([NH:7][C:8]([NH2:10])=[S:9])=[CH:5][C:4]([CH3:11])=[N:3]1.[CH3:12][I:13]>>[IH:13].[CH3:1][N:2]1[C:6]([NH:7][C:8](=[NH:10])[S:9][CH3:12])=[CH:5][C:4]([CH3:11])=[N:3]1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 12763851HCID 12763851, compound

Product 1

HCID 178504016HCID 178504016, compound

Procedure

(1,3-Dimethyl-5-pyrazolyl) thiourea (17.0 g) and 14.2 g methyl iodide were reacted as described in Example V to give 18.0 g. of the product, mp 158°-161° C.

Workup

  1. customto give 18.0 g

Sources & evidence

ORD record
ord-647cb86a850147b39355707c980f448a
Source dataset
uspto-grants-1980_10
Patent number
US04226773

Reaction notes

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