Chlorine → HCID 70591660, compound

HRID 903052Notes

Reaction equation

HRID 903052 reaction equation
[CH3:1][N:2]1[C:6]([NH:7][C:8]2[NH:9][CH2:10][CH2:11][N:12]=2)=[CH:5][CH:4]=[N:3]1.[Cl:13]Cl>C(O)(=O)C>[ClH:13].[Cl:13][C:5]1[CH:4]=[N:3][N:2]([CH3:1])[C:6]=1[NH:7][C:8]1[NH:9][CH2:10][CH2:11][N:12]=1

Participants

4

Reactant 2

HCID 24526ChlorineHCID 12763813HCID 12763813, compound

Product 1

HCID 70591660HCID 70591660, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

2(1-Methyl-5-pyrazolyl) amino-2-imidazoline (15.74 g.) was treated with 2.60 g. chlorine gas in 30 ml. acetic acid, while cooling in ice, by the method of Example VII to give 6.34 g. mp 254°-257°.

Workup

  1. customto give 6.34 g

Sources & evidence

ORD record
ord-d51c0e5d70404e8595cc414ea5e16191
Source dataset
uspto-grants-1980_10
Patent number
US04226773

Reaction notes

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