Methyl Isocyanate → HCID 178485936, compound

HRID 903222Notes

Reaction equation

HRID 903222 reaction equation
[NH:1]1[CH:5]=[CH:4][C:3]([CH2:6][NH:7][CH2:8][CH2:9][NH2:10])=[N:2]1.[CH3:11][N:12]=[C:13]=[O:14]>>[CH3:11][NH:12][C:13]([NH:10][CH2:9][CH2:8][NH:7][CH2:6][C:3]1[CH:4]=[CH:5][NH:1][N:2]=1)=[O:14]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 178511340HCID 178511340, compound

Product 1

HCID 178485936HCID 178485936, compound

Procedure

N-(3-Pyrazolylmethyl)ethylenediamine is reacted with methyl isocyanate by the procedure of Example 24 to give, after concentrating and separating the residue by column chromatography, the title compound.

Workup

  1. customto give
  2. concentrationafter concentrating
  3. customseparating the residue by column chromatography

Sources & evidence

ORD record
ord-e0c2d8750f9b4d1aaf8b8d41f457a0ae
Source dataset
uspto-grants-1980_10
Patent number
US04226874

Reaction notes

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