Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 2,4-Dichloro-6-(dimethylamino)-1,3,5-triazine | HCID 16985 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | Dichlorotriazine | HCID 18348308 | — |
| 생성물 | 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine | HCID 23338142 | — |
반응 단계
A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C.) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04226990 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-66b37f85eaa14fb1b300dbb4ab41495e |
| 출처 메모 | uspto-grants-1980_10 |