Methyl 5-bromovalerate → 5,5-Diphenylhydantoin

HRID 903325노트

반응식

HRID 903325 반응식
[C:1]1([C:7]2([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[NH:11][C:10](=[O:12])[NH:9][C:8]2=[O:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Na].BrCCCCC(OC)=O>>[CH:17]1[CH:18]=[CH:19][C:14]([C:7]2([C:1]3[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=3)[NH:11][C:10]([OH:12])=[N:9][C:8]2=[O:13])=[CH:15][CH:16]=1

참가 물질

3

반응물 2

HCID 79557Methyl 5-bromovalerateHCID 97955475,5-Diphenylhydantoin sodium

생성물 1

HCID 17755,5-Diphenylhydantoin

실험 절차

Following the method of Cook et al, Res, Comm. Chem. Path, Pharm. 5:767(1973), sodium diphenylhydantoin is reacted with methyl 5-bromovalerate followed by acid hydrolysis to yield the following: ##STR19##

후처리

  1. customfollowed by acid hydrolysis
  2. customto yield the following: ##STR19##

출처 및 근거

ORD 기록
ord-de1ed61f4b844e5794777c8825ab2d95
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04226993

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