HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl cyano(2,2,6,6-tetramethylpiperidin-4-ylidene)acetate → Cyano(2,2,6,6-tetramethylpiperidin-4-yl)acetic acid, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl cyano(2,2,6,6-tetramethylpiperidin-4-ylidene)acetate | HCID 712423 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Cyano(2,2,6,6-tetramethylpiperidin-4-yl)acetic acid, ethyl ester | HCID 6420920 | — |
Reaction Steps
This ester is hydrogenated over Pd/C in ethanol and gives ethyl 2-(2,2,6,6-tetramethyl-4-piperidinyl)-cyanoacetate which has a melting point of 116°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226999 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-6768b0ba28304cae8bf3d97b4b9201b2 |
| Source note | uspto-grants-1980_10 |