HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20475788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Hexamethylphosphoramide | HCID 12679 | — |
| Reactant | HCID 23696423 | HCID 23696423 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20475788 | HCID 20475788 | — |
Reaction Steps
A mixture of 89.0 g. of epichlorohydrin, 92.0 g. of sodium 4-(8-cyclohexyloctylamino)benzoate, and 350 ml. of hexamethylphosphoramide is stirred at 105° C. for 5 hours, allowed to cool, and poured into 1.0 liter of water. The white solid is collected by filtration, recrystallized from acetonitrile and then from hexane-methylene chloride to yield the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04227014 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-4e6b6f186c8f407892c3a91641c6a5b5 |
| Source note | uspto-grants-1980_10 |