HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54401228, compound → HCID 54557715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54401228 | HCID 54401228 | — |
| Reactant | HCID 178418634 | HCID 178418634 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 54557715 | HCID 54557715 | — |
Reaction Steps
A mixture of 2.57 g. of 1-(3-benzoylacryloyl)-L-proline, 1.42 ml. of thioacetic acid and 30 ml. of carbon tetrachloride is stirred for one hour and then concentrated in vacuo to an amber gum. This gum is dissolved in dichloromethane and the solvent removed in vacuo several times giving the desired product as an off-white glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226775 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-a6e95541f3ed4647925f82f48afe7df8 |
| Source note | uspto-grants-1980_10 |