Thioglycolic Acid → HCID 53720533, compound
Reaction equation
[C:1]([CH:9]=[C:10]([CH3:21])[C:11]([N:13]1[CH2:20][CH2:19][CH2:18][C@H:14]1[C:15]([OH:17])=[O:16])=[O:12])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[SH:22][CH2:23][C:24]([OH:26])=[O:25]>>[C:1]([CH2:9][C:10]([S:22][CH2:23][C:24]([OH:26])=[O:25])([CH3:21])[C:11]([N:13]1[CH2:20][CH2:19][CH2:18][C@H:14]1[C:15]([OH:17])=[O:16])=[O:12])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
As for Example 76, 1-(3-benzoyl-2-methylacryloyl)-L-proline is reacted with mercaptoacetic acid to give the product of the example as a glass.
Workup
- customto give the product of the example as a glass
Sources & evidence
- ORD record
- ord-72b1e1615b604e1b8004e01c9d80817b
- Source dataset
- uspto-grants-1980_10
- Patent number
- US04226775
Reaction notes
Loading…